Structural and optical properties of burr-like CuS/Cu9S 5 microwires and Cu9S5 microspheres synthesized by a two-step solvothermal method

Libo Fan; Tuanhui Feng; Peng Wang; Chunli Zhang; Zhibo Feng

doi:10.1246/bcsj.82.1015

Structural and optical properties of burr-like CuS/Cu₉S ₅ microwires and Cu₉S₅ microspheres synthesized by a two-step solvothermal method

Libo Fan, Tuanhui Feng, Peng Wang, Chunli Zhang, Zhibo Feng

Research output: Contribution to journal › Article › peer-review

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Abstract

Burr-like Cus/₉S₅ microwires and Cu₉S ₅ microspheres can be synthesized by a two-step solvothermal method. Experiment results indicated that the CuS/Cu₉S₅ microwires (diameter of ca. 300 nm and length of several micrometers) and Cu ₉S₅ microspheres (diameter of ca. 800 nm) obtained by this method had uniform morphologies and large product. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HR-TEM), and field-emission scanning electron microscopy (FE-SEM) experiments were carried out to characterize them. Fourier transform infrared (FT-IR) spectra and thermogravimetric analysis (TGA) experiments were carried out to study the components and thermal stabilization of the precursors. A possible formation mechanism and ultraviolet-visible (UV-vis) absorption spectra are also described inthis paper.

Original language	English
Pages (from-to)	1015-1022
Number of pages	8
Journal	Bulletin of the Chemical Society of Japan
Volume	82
Issue number	8
DOIs	https://doi.org/10.1246/bcsj.82.1015
State	Published - 2009
Externally published	Yes

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title = "Structural and optical properties of burr-like CuS/Cu9S 5 microwires and Cu9S5 microspheres synthesized by a two-step solvothermal method",

abstract = "Burr-like Cus/9S5 microwires and Cu9S 5 microspheres can be synthesized by a two-step solvothermal method. Experiment results indicated that the CuS/Cu9S5 microwires (diameter of ca. 300 nm and length of several micrometers) and Cu 9S5 microspheres (diameter of ca. 800 nm) obtained by this method had uniform morphologies and large product. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HR-TEM), and field-emission scanning electron microscopy (FE-SEM) experiments were carried out to characterize them. Fourier transform infrared (FT-IR) spectra and thermogravimetric analysis (TGA) experiments were carried out to study the components and thermal stabilization of the precursors. A possible formation mechanism and ultraviolet-visible (UV-vis) absorption spectra are also described inthis paper.",

author = "Libo Fan and Tuanhui Feng and Peng Wang and Chunli Zhang and Zhibo Feng",

year = "2009",

doi = "10.1246/bcsj.82.1015",

language = "English",

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T1 - Structural and optical properties of burr-like CuS/Cu9S 5 microwires and Cu9S5 microspheres synthesized by a two-step solvothermal method

AU - Fan, Libo

AU - Feng, Tuanhui

AU - Wang, Peng

AU - Zhang, Chunli

AU - Feng, Zhibo

PY - 2009

Y1 - 2009

N2 - Burr-like Cus/9S5 microwires and Cu9S 5 microspheres can be synthesized by a two-step solvothermal method. Experiment results indicated that the CuS/Cu9S5 microwires (diameter of ca. 300 nm and length of several micrometers) and Cu 9S5 microspheres (diameter of ca. 800 nm) obtained by this method had uniform morphologies and large product. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HR-TEM), and field-emission scanning electron microscopy (FE-SEM) experiments were carried out to characterize them. Fourier transform infrared (FT-IR) spectra and thermogravimetric analysis (TGA) experiments were carried out to study the components and thermal stabilization of the precursors. A possible formation mechanism and ultraviolet-visible (UV-vis) absorption spectra are also described inthis paper.

AB - Burr-like Cus/9S5 microwires and Cu9S 5 microspheres can be synthesized by a two-step solvothermal method. Experiment results indicated that the CuS/Cu9S5 microwires (diameter of ca. 300 nm and length of several micrometers) and Cu 9S5 microspheres (diameter of ca. 800 nm) obtained by this method had uniform morphologies and large product. X-ray diffraction (XRD), high-resolution transmission electron microscopy (HR-TEM), and field-emission scanning electron microscopy (FE-SEM) experiments were carried out to characterize them. Fourier transform infrared (FT-IR) spectra and thermogravimetric analysis (TGA) experiments were carried out to study the components and thermal stabilization of the precursors. A possible formation mechanism and ultraviolet-visible (UV-vis) absorption spectra are also described inthis paper.

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JO - Bulletin of the Chemical Society of Japan

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Structural and optical properties of burr-like CuS/Cu9S 5 microwires and Cu9S5 microspheres synthesized by a two-step solvothermal method

Abstract

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Structural and optical properties of burr-like CuS/Cu₉S ₅ microwires and Cu₉S₅ microspheres synthesized by a two-step solvothermal method