Preparation and sintering of zirconia ultrafine powders stabilized with scandia

Chiming Wu, Peng Wang, Zhizhou Yang, Chengwen Sun

Research output: Contribution to journalArticlepeer-review

Abstract

Nanometer zirconia ultrafine powders stabilized with scandia were prepared by chemical co-precipitation. The powders and their sintered specimens were studied by means of XRD, TEM, SEM and BET specific surface area techniques. It shows that zirconia powders stabilized with 6.0mol%, 7.8mol% and 9.6mol% scandia have good sinterability, while the specimens stabilized with 3.5mol% and 12.0mol% scandia are softly sintered, which is attributed to the existence of dual microstructure and the volume change resulting from phase transitions when the specimens are cooled from sintering temperature. In order to obtain Zirconia solid electrolyte composed of simple and stable phases, the content of scandia near 7.8mol% should be selected.

Original languageEnglish
Pages (from-to)252
Number of pages1
JournalWuji Cailiao Xuebao/Journal of Inorganic Materials
Volume11
Issue number2
StatePublished - 1996
Externally publishedYes

Keywords

  • Chemical co-precipitation
  • Nanometer ultrafine powders
  • Sintering
  • Solid electrolyte
  • Zirconia stabilized with scandia

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