TY - JOUR
T1 - [Aib5,6-D-Ala8]-cyclolinopeptide A, grown from a benzene/acetonitrile mixture.
AU - Saviano, M.
AU - Rossi, F.
AU - Filizola, M.
AU - Di Blasio, B.
AU - Pedone, C.
PY - 1995/4/15
Y1 - 1995/4/15
N2 - cyclo-(Prolyl-prolyl-phenylalanyl-phenylalanyl- alpha-aminoisobutyryl-alpha-aminoisobutyryl-isoleucyl-D-alan yl-valyl) ([Aib5,6-D-Ala8]-cyclolinopeptide A), grown from benzene/acetonitrile mixture, crystallizes with one acetonitrile and two water molecules. The molecular structure is almost identical to that obtained from methanol/water. The dimension of the solvent channels found in these structures is reduced in the present one, but the intramolecular hydrogen-bond pattern is preserved. The Pro1-Pro2 peptide unit is cis (omega = 8 degrees); all others are trans.
AB - cyclo-(Prolyl-prolyl-phenylalanyl-phenylalanyl- alpha-aminoisobutyryl-alpha-aminoisobutyryl-isoleucyl-D-alan yl-valyl) ([Aib5,6-D-Ala8]-cyclolinopeptide A), grown from benzene/acetonitrile mixture, crystallizes with one acetonitrile and two water molecules. The molecular structure is almost identical to that obtained from methanol/water. The dimension of the solvent channels found in these structures is reduced in the present one, but the intramolecular hydrogen-bond pattern is preserved. The Pro1-Pro2 peptide unit is cis (omega = 8 degrees); all others are trans.
UR - http://www.scopus.com/inward/record.url?scp=0029644495&partnerID=8YFLogxK
U2 - 10.1107/s0108270194006864
DO - 10.1107/s0108270194006864
M3 - Article
C2 - 7619339
AN - SCOPUS:0029644495
SN - 0108-2701
VL - 51 ( Pt 4)
SP - 663
EP - 666
JO - Acta crystallographica. Section C, Crystal structure communications
JF - Acta crystallographica. Section C, Crystal structure communications
ER -